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Marine Borer Resistance of Acetylated and Furfurylated Wood – Results from up to 16 years of Field Exposure
2016 - IRG/WP 16-40756
Furfurylated and acetylated Scots pine sapwood has been tested since 1999 in a marine field with high marine borer activity. In 2004, two test groups with acetylated southern yellow pine (product later known as Perennial Wood™) were put out and over the whole test period differently furfurylated wood (later marketed as Kebony®) test groups have been started. Furthermore, some combinations of mo...
M Westin, P Larsson Brelid, T Nilsson, A O Rapp, J P Dickerson, S Lande, S Cragg
Accelerated weathering and fungal resistance of wood modified with isopropenyl acetate
2016 - IRG/WP 16-40764
Chemical modification of Rubberwood (Heveabrasiliensis Müll.Arg) with isopropenyl acetate (IPA) in presence of anhydrous aluminum chloride and iodine as catalysts was carried out. Modified wood surfaces were exposed to UV light source in an accelerated weathering tester to evaluate UV resistance. Anti-swelling efficiency (ASE) and fungal resistance of modified wood were also evaluated. Modified w...
G B Nagarajappa, K K Pandey
State of the art of industrial wood protection in Portugal
2016 - IRG/WP 16-30703
This work intended to give a perspective of industrial wood protection in Portugal. A survey was made of the companies treating wood mainly for use classes 3 and 4 such as autoclave treatments with biocides and wood modification procedures. Currently there are 23 companies with 33 production plants with an autoclave installed for wood preservation by impregnation. There are also two companies prod...
L Nunes, J Carmo, J Vicente, B Esteves
Moisture content as a quality control parameter in thermally modified timber production
2017 - IRG/WP 17-20622
Quality assurance (QA) or factory production control (FPC) is necessary to ensure a proper production process. The requirements of QA/FPC can result from EN and national standards, quality assurance systems, or producer-specific rules.
TMT producers must ensure that the process was correct, and to ensure traceability of products. In addition to the electronic records, the material should be che...
W Scheiding, H Turkulin, S Stein
New Standards for Approval of Modified Wood within the Nordic Wood Preservation Council (NWPC)
2017 - IRG/WP 17-20624
In the Nordic countries, there is a long tradition for quality labelling of preservative treated wood. Until now the labelling has been restricted to pine and other easy to treat wood species, but with the introduction of a new set of standards it is now possible to obtain the Nordic Wood Preservation Council’s (NWPC) quality labelling also for modified wood.
In this paper, we will introduce th...
N Morsing, E Engelund Thybring, M Klamer
Effects of Nano-Wollastonite Impregnation on Fire Properties of Some Thermally-Treated Solid Wood Species
2017 - IRG/WP 17-40771
The effects of nano-wollastonite (NW) suspension impregnation on the fire-retarding properties of heat-treated solid wood of three species (beech, poplar, fir) were studied. Heat treatment was performed at two temperatures of 180 °C and 200 °C. Impregnation was carried out at a pressure of 3 bars for 30 min. The fire properties included ignition time, glowing time, back-darkening, back-splitting...
H R Taghiyari, R Hossinpourpia, S Adamopoulos, A Jahangiri, D Rabie
Commercialisation of DMDHEU Modified Wood in Australasia
2017 - IRG/WP 17-40772
While there is an increasing volume of data for the impregnation and curing of timber using dimethylol dihydroxyethyleneurea (DMDHEU) on species such as Scots Pine, Beech, Slash Pine and Spotted gum, there is limited information available on the impact of the modification process on the performance of Pinus radiata (referred to hence forth as Radiata pine). The variability within material and spec...
B R Derham, T Singh, H Militz
Accessibility of hydroxyl groups in anhydride modified wood as measured by deuterium exchange
2017 - IRG/WP 17-40784
Acetylated wood shows improved properties largely due to the reduced amount of water in the acetylated cell wall. However, the exact mechanism by which water is excluded in acetylated wood remains unclear. Acetylation reduces hydroxyl content by substitution of hydroxyl groups in wood polymers but may also hinder access to unmodified hydroxyls by physical bulking. This work assesses hydroxyl acces...
G Beck, S Strohbusch, E Larnøy, H Militz, C Hill
Decay resistance of beams made from thermally modified Scots pine and Norway spruce after 6 years’ exposure in ground contact
2017 - IRG/WP 17-40806
In the present study the resistance of beams treated by ThermoWood® process was studied in ground contact and the results given are based on a “modified” EN 252 test. After six years’ exposure clear differences were found between untreated Scots pine and Norway spruce beams and treated ones. In all cases thermal modification improved the performance. Thermally modified pine heartwood showed...
S Metsä-Kortelainen, H Viitanen
Influence of hygro-thermal treatment temperature and duration on dimensional stabilisation of wood modified with poly(butylene succinate)
2017 - IRG/WP 17-40813
To improve wood properties, especially dimensional stability, a treatment based on poly(butylene succinate) oligomers (OBS) was experimented. After impregnation in wood, a further hygro-thermal treatment (HTT) was carried out in a pressurized reactor at 100% relative humidity (RH) at differing temperatures for differing durations. The aim of HTT is to induce partial swelling of wood cell walls so ...
C Grosse, M Noël, L Rautkari, P Gérardin
FTIR-ATR monitoring of chemical changes of thermo-chemically modified beech wood degraded by brown-rot fungus
2018 - IRG/WP 18-40823
Wood chemical modification with lactic acid oligomers (OLA) has been reported to confer promising properties for wood outdoors applications. To better understand the lactic acid interaction with wood, chemical changes following biological degradation have been characterized with a battery of tests. Fourier transform infrared (FTIR) spectroscopy has been proved to be a valuable tool for studying fu...
C Grosse, M Noël, M-F Thevenon, P Gérardin
Resistance of modified wood to termite attack assessed in laboratory and field testing: A review of internal research
2018 - IRG/WP 18-40824
Within the past decades, new wood modification technologies have been investigated in order to improve certain wood characteristics and enable the use of timber products for outdoor applications. Some of these non-biocidal technologies have been developed and commercialized recently. Thus, various material properties were studied intensively and shown to be improved. To a great extent, previous re...
L Emmerich, P Gascón-Garrido, H Militz
Thermally modified timber treated with methacrylate
2018 - IRG/WP 18-40849
Thermally modified timber (TMT) from Scots pine sapwood similar to Thermo-D quality was impregnated with methacrylate resin by the hot-and-cold method and subsequently cured at elevated temperatures. The results showed that methacrylate resin could be used to reduce colouring of painted TMT wood during accelerated weathering probably by hindering the migration of extractives. The resin itself did ...
O Karlsson, O Myronycheva, DJones, D Elustondo, D Sandberg
Hydroxyl accessibility - A brief review of deuterium exchange studies on modified wood
2019 - IRG/WP 19-20656
Wood modification imparts dimensional stability and decay resistance. The mechanism(s) by which this occurs are thought to be related to the bulking of the wood cell wall and subsequent moisture exclusion. Hence, quantification of accessible hydroxyl (OH) groups is of great interest when evaluating and increasing the understanding of the performance of modified wood. The aim of this study was to b...
G Beck, C Hill, G Alfredsen
Durability classification of preservative treated and modified wood
2019 - IRG/WP 19-20659
EN 350 (2016) allows formally to determine durability classes (DC) for wood products and wood-based materials, which was previously only possible for untreated wood in the form of natural durability. In a first study, the University of Goettingen carried out the durability classification of chemically modified (modified with 1,3-dimethylol-4,5-dihydroxyethyleneurea, DMDHEU) and preservative-treate...
S Bollmus, L Bachle, C Brischke, H Militz
Performance of modified wood in service - multi-sensor data fusion and its multi-way analysis
2019 - IRG/WP 19-20660
Recent developments in the field of electronic sensors and analytics provide new opportunity for accurate characterization of materials often based on portable and non-destructive methods. By using several complementary techniques, the material description is precise and complete. The data provided by multiple equipment, however, are often not directly comparable due to different resolution, sensi...
A Sandak, J Sandak, M Cocchi
Using X-ray scattering to elucidate the mechanisms behind the moisture and fungal decay resistance of epoxybutene modified wood
2019 - IRG/WP 19-40854
Chemical modification of the hydroxyl groups of wood can improve the properties of wood by providing moisture and biological resistance, as well as dimensional stability. Southern pine solid wood was chemically modified to various weight percentage gains (WPG) with epoxybutene (EpB, 8%-38% WPG). After modification, specimens were extracted with a toluene: ethanol (2:1) solution for 2 hours or wate...
R E Ibach, N Plaza
Dimensional stability and decay resistance of montmorillonite- furfuryl alcohol modified wood
2019 - IRG/WP 19-40856
Poplar (Populus cathayana) wood was impregnated successively by organo-montmorillonite (OMMT; in concentration of 2%) and furfuryl alcohol (FA, in concentrations of 15%, 30% and 50%) in a two-step method to prepare OMMT-FA modified wood. The modified wood samples were characterized using X-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM). Moreover, wood physical and a...
L Zhang, J Cao
Study on the ability of wood-destroying fungi to grow through chemically modified wood
2019 - IRG/WP 19-40858
Over the last decades, chemical wood modification technologies were developed to increase the resistance against attack by wood-destroying organisms without using biocides. Most of those technologies are based on an impregnation step initially. In most treated wood products, mainly by using solid wood in thicker dimensions as in posts, poles, sleepers, deckings etc. it is known that wood impregnat...
L Emmerich, S Strohbusch, C Brischke, S Bollmus, H Militz
Novel approaches for improvement of dimensional, photo- and thermal stability of wood through liquefied wood polyols impregnation
2019 - IRG/WP 19-40884
The major problems encountered in both indoor and outdoor utilization of wood are due photo instability and dimensional instability. The modification of Melia dubia wood for ultraviolet resistance and dimensional stability with liquefied wood has been carried out through impregnation method under solvent free conditions. The level of impregnation in modified wood was estimated by weight perc...
A Kumar, A John, T S Mehra
Studying amount, location and state of water in modified wood at moisture levels relevant for fungal degradation
2020 - IRG/WP 20-40889
Water is an essential parameter for fungal degradation of wood, but degradation primarily occurs at high moisture levels at water potential in the range of -4 to -0.1 MPa, which corresponds to 97-99.9% relative humidity. At these moisture levels, water is present in the wood structure both in and outside of cell walls. The majority of previous studies on the interaction between wood and water for ...
M Fredriksson, E Engelund Thybring, Ramunas Digaitis
Elucidation of reactive sites of wood modified with acetic anhydride: Insights from density functional theory calculations
2020 - IRG/WP 20-40892
Density functional theory (DFT) was employed to investigate the interaction of cellulose and lignin with acetic anhydride for explaining the wood modification process. Atoms in molecules (AIM) and reduced density gradient (RDG) along with non-covalent interaction (NCI) plots were used to analyse the intermolecular bonding characteristics. Cellulose was modelled with a cellobiose unit (dimer of glu...
V Ponnuchamy, A Sandak, J Sandak, R Herrera Diaz
Development of procedures for sampling, testing, and classification to determine the biological durability of wood and wood products
2020 - IRG/WP 20-20676
This paper informs about a research project, which deals with several shortcomings and a lack of clarity within EN 350:2016. The project started in January 2020, will run for 3 years, and is operated by the Institute of Wood Technology Dresden (IHD) and the University of Goettingen (UGOE).
Determination and classification of durability of wood and wood products against wood-destroying organisms ...
W Scheiding, K Jacobs, S Bollmus, C Brischke
Performance of resin-treated solid wood and laminated veneer lumber (LVL) under marine conditions
2021 - IRG/WP 21-10973
Wood is a traditional building material in the marine environment, where it is exposed to extremely harsh conditions. Most of the indigenous softwood and hardwood species in Europe are not durable against attack by marine organisms. Recently, wood modification has been considered as an alternative to protect non-durable wood species under use class (UC) 5 (EN 335, 2013) conditions. The present stu...
L Emmerich, C Brischke, S Bicke, H Militz
Experience Experience from over 20 years of field trials of resin treated wood – Marine borer resistance of MMF and DMDHEU modified wood
2021 - IRG/WP 21-10976
In 1999 a field test of Scots pine treated with MMF (Methylated Melamine Formaldehyde) resin and acetylated Scots pine post treated with MMF resin was started. Six years later a commissioned full NWPC test for BASF of Belmadur® (DMDHEU resin treated wood) was started at the same site.
The testing, according to European Standard EN 275, was done in a bay by Kristineberg Marine Research Station o...
M Westin, P Larsson Brelid, A O Rapp, J Habicht