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Full-scale impregnation of wood with siloxane using supercritical carbon dioxide
2014 - IRG/WP 14-40659
Full-scale impregnation of wood with siloxane was carried out using supercritical carbon dioxide as solvent. A batch of 3530 kg of Scots pine sapwood was impregnated to a retention of approximately 1.3% siloxane. The treatment also consisted of a simultaneous impregnation with organic biocides. The performance of the wood was evaluated in terms of capillary water uptake according to a modified EN ...
A Kjellow, F Imsgard, J Fernandes, R Wagner, J Delis


Improving dimensional stability of thermally treated wood by secondary modification – potential and limitations
2014 - IRG/WP 14-40664
The potential of treating thermally modified wood with melamine resin to improve the dimensional stabilization is tested in this research. Two different boards of poplar (Populus ssp.) were cut into two halves. One half of each board was thermally modified (T1 and T2) in a commercial process, the other half was used as untreated reference material. The material was thermally modified using the vac...
G Behr, K-C Mahnert, S Bollmus, H Militz


Development of new wood treatments combining boron impregnation and thermo modification - Effect on decay and termites durability
2014 - IRG/WP 14-40666
Environmental pressures appeared in most European countries during the last decade has lead to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative methods during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important chemical mo...
S Salman, A Pétrissans, M-F Thévenon, S Dumarçay, B Pollier, P Gérardin


Functional silicones used as a potential tool for the development of non-biocidal wood treatments
2015 - IRG/WP 15-30665
The increase of wood resistance against biological agents for outdoor use is conventionally performed by deep impregnation with preservatives. However, some of the traditional wood preservatives, used for decades for wood protection and regarded as the most effective, are currently subjected to severe restrictions because of their toxicity. In fact, new preservation technologies are constantly ent...
F Lhumeau, C Delaite, F Marchal, F Pochon, M Kutnik


Characterization of biofilm formation on wood treated with vegetable oils by color-based image interpretation method
2015 - IRG/WP 15-40697
The protection of wood in order to extend its service life is an important issue nowadays. As an alternative to traditional wood coatings biofilms can be used. It is a living protective coating for the wood surface against UV and bio-degradation that has the ability to recover from local damage, such as cracks. This paper presents preliminary results of biofilm formation from an 8-month’s fie...
K Filippovych, H Huinink, L van der Ven, O C G Adan


Accelerated Weathering Performance of Impregnated Wood Samples Coated with Zinc by Means of Plasma-Assisted Particle Deposition
2016 - IRG/WP 16-30682
Many different methods are currently applied for wood protection against outdoor conditions. The most important of these is the process of impregnation with liquid substances. However, this kind of wood preservatives cannot provide a long-term protection of wooden surfaces. Weathering-resistant surfaces can be obtained by applying UV absorbing agents. In this study, the influence of zinc particles...
A Can, H Sivrikaya


The termite resistance of wood impregnated with nano-zinc oxide and nano-zinc borate dispersions
2016 - IRG/WP 16-30691
In this work, the effects of the impregnation with nano-ZnO and nano-ZnB dispersions on the termite resistance of European beech wood were investigated. Three different concentrations (namely 0.5%, 1% and 2%) of the above two materials were tested. Water leaching effect was also investigated. It was concluded that a severe effect in terms of termite workers mortality is induced by the use of both ...
C Lykidis, T de Troya, M Conde, J Galván, G Mantanis


Modifying wood with paraffin wax emulsion impregnation and thermal modification: hydrophobization effect and mechanism of the combined treatment
2016 - IRG/WP 16-40726
The aim of this study was to enhance the water repellency of wood by a combined treatment of paraffin wax emulsion (PWE) impregnation and thermal modification. Two different treating procedures were used to modify the southern pine (pinus spp.). One is first PWE impregnation and then thermal modification, another is first thermal modification and then PWE impregnation. The treated samples were imm...
Wang Wang, Jinzhen Cao, Cong Chen


Impregnation of railway sleepers - Pressure gradient and transversal penetration
2016 - IRG/WP 16-40731
Based on the possible ban of creosote in the future, the need for oil based alternative products has gained in importance. Due to possible differences in impregnation properties compared to creosote the need for re-implementing former technology is given, to determine if momentarily used impregnation processes have to be modified. The here reported tests measure the pressure gradient during the im...
M Starck, A Gellerich, H Militz


Dynamic mechanical analysis of viscoelastic properties of heat treated glycerol-impregnation poplar wood
2016 - IRG/WP 16-40732
The viscoelastic properties of glycerol-impregnated poplar wood after heat treatments at various temperatures were examined by dynamic-mechanical analysis. The spectra of storage modulus (E’) and loss tangent (tgδ) in the frequency at 10 Hz were measured at the temperature range from -100 to 300℃. Compared to no peak in E’ spectra and two relaxation processes in tanδ spectra of...
Li Yan


Influence of pressure phase impregnation time on the uptake and distribution of wood preservatives in Scots pine material of diverse treatability
2016 - IRG/WP 16-40752
In spite of the general opinion that Scots pine sapwood is easy to impregnate considerable variations in treatability are reported. In order to study impregnation results of diverse Scots pine sapwood treated with increasing process times, Scots pine sapwood from two different predefined treatability groups was impregnated. A copper solution was used as impregnation agent in ten different vacuum p...
K Zimmer, B Kerfriden


Improvement of wood properties by impregnation with liquefied spruce bark based resins
2016 - IRG/WP 16-40761
In this paper, biobased phenolic thermosetting resins are designed to be used as wood stabilization treatment. The originality of the study stands in substituting part of phenol by spruce (picea abies) bark: this is achieved by a liquefaction process in phenol in the presence of sulfuric acid as catalyst. Next, thermosetting resins are synthetized from liquefied bark by condensation on formaldehy...
X Duret, E Fredon, E Masson, P Gérardin


Development of Wood Modification – High melting point wax and hot oil treatments
2016 - IRG/WP 16-40768
This study covers an introduction to the projects where new facilities were created for developing wood modification. In this new research environment it is possible to treat wood with versatile equipment. First modifications with this equipment are going to be done in high temperature and pressure using high melting point waxes and hot oils. Earlier studies, tests and commercial products show...
H Turunen, L Linkosalmi, J Peura, O Paajanen


Quality of the impregnated wood in the Slovenian hardware stores
2017 - IRG/WP 17-20606
Ten different samples from Slovenian hardware stores were analysed. Samples were treated with copper based wood preservatives and designed and advertised to be used in heavy duty applications in use classes 3.2 or 4. In order to determine the quality of the treatment penetration, retention and fungicidal properties were determined. Retention was determined with XRF analysis, while modified EN 113 ...
M Humar, B Lesar, N Thaler, D Kržišnik, N Kregar, S Drnovšek


Effects of Nano-Wollastonite Impregnation on Fire Properties of Some Thermally-Treated Solid Wood Species
2017 - IRG/WP 17-40771
The effects of nano-wollastonite (NW) suspension impregnation on the fire-retarding properties of heat-treated solid wood of three species (beech, poplar, fir) were studied. Heat treatment was performed at two temperatures of 180 °C and 200 °C. Impregnation was carried out at a pressure of 3 bars for 30 min. The fire properties included ignition time, glowing time, back-darkening, back-splitting...
H R Taghiyari, R Hossinpourpia, S Adamopoulos, A Jahangiri, D Rabie


Penetration behaviour of different hydrophobic carrier substances for oily wood preservatives in Beech and Scots pine sapwood
2017 - IRG/WP 17-40804
The use of creosote as a wood preservative has a long history. Current areas of application are railway sleepers, transmission poles, timber bridges and marine applications. If the approval for creosote will not be prolonged, alternative wood preservatives will be needed. As the penetration behaviour after pressure impregnation of different alternative oily products in this fields of application i...
M Starck, A Gellerich, H Militz


Organosilicon-based impregnation hydrophobers for wood
2017 - IRG/WP 17-40808
The SILEX project “Improving sustainability of construction materials using innovative Silicon based treatment” is a Life+ project with reference LIFE+11 ENV/BE/1046 and started in April 2013. This project intends to demonstrate that a new class of compounds can be used for wood treatment for an extended service life combined with enhanced new testing methodology. The project aims at demonstra...
J-P Lecomte, J Van Acker, J Van den Bulcke, M Kutnik, M Montibus, S Salvati, S Derocker


Mineralization of European oak with various ionic salt solutions to achieve an in situ precipitation of calcium oxalate
2019 - IRG/WP 19-40861
Thin specimens of European oak (Quercus spp.) with the dimensions of 4 × 20 × 50 mm3 were treated with various aqueous ionic salt solutions of calcium chloride, potassium oxalate and calcium acetate. Additionally, the oak was treated with combinations of calcium chloride and potassium oxalate, as well as calcium acetate and potassium oxalate with the aim to precipitate in situ the water insolubl...
T Franke, T S Volkmer


Improvement of wood decay and termite durability resulting from combined treatments based on borax/phenol-formaldehyde impregnation followed by thermal modification
2019 - IRG/WP 19-40871
This study determined the factors influencing the boron content after leaching of pine blocks impregnated with aqueous solution of phenol-formaldehyde (PF) resin with or without borax and subjected to heat treatment by response surface methodology. An experimental design permits to analyze the effects of heat treatment temperature (150, 185 and 220°C), curing time (5, 12, 5 and 20 hours), resin c...
S Salman, M-F Thevenon, A Petrissans, S Dumarcay, P Gerardin


Promoting Commercially Available Epoxy Resins for Non-biocidal Wood Preservation
2019 - IRG/WP 19-40877
Commercially available epoxy and polyamine resins were evaluated with the aim of developing new non-biocidal wood preservation treatments. A simple method allowing the impregnation of wood by vacuum double impregnation followed by a curing process was developed for two reference species, beech Fagus sylvatica and Scots pine Pinus sylvestris. The tested products were evaluated for their ability to ...
P Poveda, M Mubarok, S Dumarcay, M Montibus, I Le Bayon, M Kutnik, P Gerardin, F Simon


Novel approaches for improvement of dimensional, photo- and thermal stability of wood through liquefied wood polyols impregnation
2019 - IRG/WP 19-40884
The major problems encountered in both indoor and outdoor utilization of wood are due photo instability and dimensional instability. The modification of Melia dubia wood for ultraviolet resistance and dimensional stability with liquefied wood has been carried out through impregnation method under solvent free conditions. The level of impregnation in modified wood was estimated by weight perc...
A Kumar, A John, T S Mehra


Evaluation of chemical densification of three hardwood species through in-situ electron beam polymerization
2020 - IRG/WP 20-40893
Hardwoods are the most suitable species for wood flooring for their appearance as well as their hardness. Yet, improving hardness can provide substantial benefit for the wood flooring market. Chemical densification of wood and in-situ polymerization through electron beam technology was chosen to increase hardness of three hardwoods (Yellow birch (YB) (Betula alleghaniensis Britt.), Sugar maple (SM...
J Triquet, P Blanchet, V Landry


Impregnation of railway sleepers - Investigation of a system-sleeper as an alternative for creosote treated sleepers
2020 - IRG/WP 20-40896
For nearly 200 years wooden railway sleepers are impregnated with creosote. After initially using vacuum pressure processes for impregnation, empty-cell processes have been developed quickly and are used until today. Because of political developments, creosote will probably be banned on the European market in the near future. The Fürstenberg-System-Sleeper, which combines for Europe innovative as...
M Starck, A Heidel, C Brischke, H Militz


Monitoring uptake and penetration of pesticides during impregnation of pine (Pinus sylvestris) and spruce (Picea abies) wood with bio-based microemulsion gel formulations
2020 - IRG/WP 20-30756
Even in dry state wood is susceptible to biological degradation. Preservation against biological decay in exposed conditions is conventionally achieved by impregnating the wood with pesticides applied at professional and industrial levels. Impregnation of wood with preservatives is a complex process that involves wood macro- and microstructure, and the physical characteristics of woods. Here we fo...
D Messaoudi, K Ruel, J-P Joseleau


NewSiest-Enhancement of UV stability of thermally modified wood through envelope impregnation with nanobased stabilisers
2020 - IRG/WP 20-40909
Thermal modification is a process which improves the properties of wood, resulting in a material that can be disposed at the end of the product life cycle without presenting an environmental hazard. Thermally modified wood retains as a natural product and the grain, original colour variances and characteristics of wood are still present. However, exposure to daylight causes brightening or greying ...
K Srinivasa, M Petrič


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