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Gene expression analysis of a copper-tolerant brown rot fungus on MCQ-treated wood
2011 - IRG/WP 11-10748
Most brown rot fungi are copper-tolerant, which makes them difficult to control with copper-based wood preservatives like MCQ. To better understand what biological processes are regulated, we used our model species, Antrodia radiculosa, to examine expression of genes on MCQ-treated wood. Our hypothesis was genes that decreased copper bioavailability would be up-regulated early, when wood showed ...
J D Tang, A Perkins, S V Diehl


Comparative investigations between thermal and microwave assisted digestion as a novel tool for the chemical analysis of inorganic wood preservative components
2011 - IRG/WP 11-20461
The correct chemical impregnation of wood requires an internal as well as external quality control of the treated wood. The active is located in a solid matrix, therefore it is often difficult to analyse such material since most analytical procedures are based on liquid systems. Because of this quite a number of methods – like extraction or thermal digestion - were developed in order to transfer...
H Ahl, J Fromm, E Melcher


Classification of wood materials using Fourier Transform Near Infrared Spectroscopy and multivariate analysis
2011 - IRG/WP 11-20471
A distinction between preservative-treated wood and non-treated wood can be demonstrated by the combination of Fourier Transform-Near Infrared Spectroscopy (FT-NIRS) and Multivariate Analysis (MVA). This technique is non-destructive, quick, easy to use and can be portable. The calibration models for different heavy metals are set up using principal component analysis (PCA) to classify species of t...
M A Bouslamti, M A Irle, C Belloncle, V Salvador, S Hulot, B Caron, E M Qannan


A comparative study and evaluation of methodologies used for determining wood preservative penetration
2011 - IRG/WP 11-20475
A series of methods for determining penetration of wood preservatives into the wood structure have been developed for either quality control (QC) or research and development purposes. QC methods range from monitoring the solution uptake, applying colour indicators or sampling specific wood samples followed by wood acid digestion/atomic absorption spectroscopy (AAS) or solvent extraction/chromatogr...
R Craciun, R Moeller, J Wittenzellner, T Jakob, J Habicht


Slice - Cut and Analyze Laser Microdissection (LMD): A method to produce sample material from modified wood for chemical quality analysis
2011 - IRG/WP 11-20478
Wood modification with its various systems is an established way to enhance a wood products’ service life in outdoor applications. Per definition, selected material properties are enhanced by means of modification without producing toxic substances or residues during service life and combustion afterwards. The systems of impregnation modification include a physical and often chemical alteration ...
K Zimmer, E Larnøy, A Treu, M Fongen


Non-destructive evaluation of wood decay
2011 - IRG/WP 11-20479
Evaluation of wood decay is often prone to subjective assessment. Standard rating scales are based on human perception of decay, often in addition to weight loss measurements. Especially the assessment of graveyard specimens or other long term testing material that has to be monitored regularly on a non-destructive basis, is challenging. In this paper two techniques are presented that can deliver ...
J Van den Bulcke, I De Windt, N Defoirdt, J Van Acker


LOSP for glulam, when should the treatment be applied?
2011 - IRG/WP 11-30555
Treatment options for outdoor above-ground (H3) exposed glulam of Pinus radiata and P. elliottii were examined. Beams were treated with azole LOSP (containing a zinc tracer) aiming for retentions of 35-40 l/m3 or 70-80 l/m3. Treatment was conducted either before or after gluing. TBTN LOSP and CCA were included as comparative treatments. Test specimens for exposure were cut after treatment, while w...
L J Cookson


Further Studies on the Distribution of Copper in Treated Wood Using an XRF Microscope Technique
2011 - IRG/WP 11-40549
There are two distinct forms of copper in aqueous copper based wood preservative systems that are currently used in the United States for treatment of southern pine lumber. These are systems using either soluble copper (typically amine based) or the more recent particulate or “micronized” copper as the primary biocide. Studies reported last year showed that there were distinct differences in...
A Zahora


Above Ground Field Evaluation and GC-MS Analysis of Naturally Durable Wood Species
2012 - IRG/WP 12-10764
Nine wood species are being evaluated in above ground field studies in Mississippi and Wisconsin. Candidate naturally durable wood (NDW) species are being rated at yearly intervals for resistance to decay, cupping, and checking. Field ratings after 12 months exposure are presented. To date, Paulownia tomentosa (PAW) and southern yellow pine (SYP) are least durable and cedars are the most durable i...
G T Kirker, A B Blodgett, S T Lebow, C A Clausen


Use of X-Ray Micro-Computed Tomography to Visualize Copper in Preservative Treated Wood
2012 - IRG/WP 12-20488
This study tests the hypothesis that X-ray micro-computed tomography will be able to visualize the distribution of copper in wood treated with a micronized wood preservative containing copper carbonate. A small wood block measuring 12 x 12 x 19 mm was cut from a 2.4 m x 51 mm x 51 mm southern pine batten that had been treated with a micronized wood preservative. Tomograms of the wood block were ob...
P D Evans, A Limaye, H Averdunk, M Turner, T J Senden, M A Knackstedt


Plywood under the scanner: linking moisture dynamics and 3D structure
2012 - IRG/WP 12-20491
Plywood is highly esteemed as a construction material. Yet, the influence of moisture on both strength and durability are important factors. Especially the dynamics of moisture desorption and absorption should be taken into account when assessing the quality of a panel, which is a fact for all panel materials. This paper therefore focuses on the monitoring of the moisture dynamics of plywood subje...
J Van den Bulcke, I De Windt, N Defoirdt, J Van Acker


Tannin resin-boron associations: Leaching and biological resistance
2012 - IRG/WP 12-30587
The easy leaching of boron in wood preservation formulations has allowed to use this fungicide only for short term applications. The recently discovered adduct with flavonoids allows boron to resist longer periods of time within wood and consequently extend its life. Two different leaching treatments were compared and the fungal and termite decay was examined. The biological tests have shown extre...
G Tondi, S Wieland, N Lemenager, A Petutschnigg, A Pizzi, M-F Thevenon


Influence of heat treatment intensity on the structural integrity of 14 timber species
2012 - IRG/WP 12-40586
Thermally modified timber (TMT) is characterized by improved durability and dimensionally stability, but strength properties, especially the dynamic ones, are compromised at the same time. Because dynamic standard tests require high efforts and time, the high-energy multiple impact (HEMI) –test was developed for the fast and reliable characterisation of the structural integrity of TMT, showing a...
C R Welzbacher, C Brischke, G Maier


Utilization of thermodesorption coupled to GC-MS to characterize volatiles formation kinetics during wood thermodegradation
2012 - IRG/WP 12-40587
Identification of volatile degradation products produced during wood mild pyrolysis is important to have better insight on thermodegradation mechanisms. Previous studies have shown that thermodesorption coupled to GC-MS is an attractive tool to characterize and quantify products formed during wood thermodegradation indicating an higher susceptibility of hardwoods to thermodegradation compare to so...
K Candelier, S Dumarçay, A Pétrissans, M Pétrissans, P Kamdem, P Gérardin


Chemical Analysis of Hydrothermally Treated Beech Wood in Buffered Mediums
2012 - IRG/WP 12-40604
Hydrothermal treatment of beech wood in buffered mediums was carried out to study the effect of different mediums of heat treatment on crystallinity index of treated specimens due to degradation of carbohydrates. Different mediums (water, buffer5, 7 and 8) and temperatures (160 and 180 °C) were used. ATR spectra focusing on indexes of carbohydrates degradation obtained and analyzed. Results showe...
A Talaei, A Karimi


Nano structural properties of La2O3-Beech Wood Flour With XRD technique
2012 - IRG/WP 12-40607
This research was considered to study various properties of the Lanthana mixed with beech wood flour (BWF), as a new structure. For this purpose, La2O3 powders in the BWF have been obtained by sol-gel method using simultaneous gelation of all cations. La2O3 - BW samples are analysed by X-ray diffraction .The obtained results showed the formation of nano crystalline La2O3 phases. The average crys...
M Ghorbani Kokandeh, I Bahamni, A Bahari


Initial investigations into the spalting potential of Peruvian hardwoods
2014 - IRG/WP 14-10813
This study was performed to determine if several moderately-utilized Peruvian hardwoods had potential for spalting applications. We applied a modified decay jar methodology with six native Peruvian woods and three moulds, with a period of incubation of six weeks. Results showed that Nigrospora sphaerica and Marupa (Simarouba amara) resulted on the highest significant internal pigmentation (black),...
S M Vega Gutiérrez, S C Robinson


Statistical analysis of durability tests - Part 1: Principles of distribution fitting and application on laboratory tests
2013 - IRG/WP 13-20504
Service life prediction is an important topic in wood research, especially with regard to the Construction Products Regulation (CPR). Both laboratory tests as well as in-service performance testing are therefore essential in combination with proper monitoring and analysis tools. A crucial concept is variability in testing and analysis, especially for a biological material such as wood. The larger ...
I De Windt, J Van den Bulcke, C Brischke, C R Welzbacher, A Gellerich, S Bollmus, M Humar,


A critical view on early indicators for above ground field performance of wood
2013 - IRG/WP 13-20509
Above ground field tests are quite often a balancing act between the provision of realistic test conditions, reliable statistics, and acceptable long test durations. Within this study we therefore reviewed 543 data sets from above ground field tests performed at 36 different test sites in 8 countries in Australia and Europe. The main objective was to investigate possible correlations between early...
C Brischke, L Meyer, G Alfredsen, P-O Flæte, L Francis, M Hansson, P Larsson Brelid, J Jermer


Statistical analysis of durability tests - Part 2: Principles of time-to-failure and application on field test data
2013 - IRG/WP 13-20512
Service life prediction is an important topic in wood research, especially with regard to the Construction Products Regulation (CPR). Both laboratory tests as well as in-service performance testing is therefore essential, in combination with proper monitoring and analysis tools. A crucial concept is variability and the incorporation of variability in tests and analysis. In this paper we focus on t...
J Van den Bulcke, I De Windt, C Brischke, C R Welzbacher, A O Rapp, J Van Acker


Image analysis for mould and sapstain detection on wood
2013 - IRG/WP 13-20519
Laboratory tests for mould growth on wood products are time consuming and rely on visual assessments of specimens utilizing subjective rating systems. Accelerated laboratory methods are needed that can provide rapid, quantitative assessment of mould and sapstain growth on solid and composite wood products. Image analysis of scanned spore imprints from southern pine or oriented strandboard (OSB) sp...
C A Clausen, V W Yang


Extraction and analysis of DNA from green and seasoned timber as basic methods for determination of wood species and origin
2013 - IRG/WP 13-20523
Against the background of the European timber trade regulation EUTR, commenced to law by March 2013, the determination of wood species and tracing of its origin is getting a great importance. A promising approach for establishing fast and reliable tracking systems for wood products is DNA analysis. A critical point is the extraction of analysable DNA from the wood and its lignified cell walls. Thu...
K Jacobs, H Mende, W Scheiding


Surface energy characterization of thermally modified wood using inverse gas chromatography
2013 - IRG/WP 13-20532
The objective of this work is to characterize surface energetics of thermally modified wood. Such information may be useful for a better understanding and predictions of adhesion properties between the modified wood and other material systems, e.g. coatings, adhesives or matrices in composites. Inverse gas chromatography (IGC) was used to study the surface energy characteristics of thermally modif...
S Källbom, K Segerholm, D Jones, M Wålinder


Visualization of Copper in the Voids and Cell Walls of Treated Wood using X-Ray Micro-Computed Tomography
2013 - IRG/WP 13-40640
This study extends our observations of the distribution of copper in treated wood. A small wood block was cut from a southern pine batten that had been treated with a particulate-copper preservative and similar sized block was cut from a batten that had been treated with a copper-amine preservative. Both blocks were imaged using X-ray micro-computed tomography. We obtained tomograms of each treate...
P D Evans, A Limaye, H Averdunk, M Turner, T J Senden


Quantification of copper and chromium in field stakes after different exposure times: Remaining metal content and distribution
2013 - IRG/WP 13-50291
In order to determine the distribution of copper and chromium as well as their remaining concentration EN 252 specimens and thicker pine sapwood stakes (non standard format) were treated with a commercial CC salt in a vacuum pressure process. The stakes were installed in the test field of the Institute of Wood Research, Hamburg, in August 2010. In all cases three stakes were removed after 4, 8, 12...
T Liese, M Bahmani, E Melcher


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