IRG Documents Database and Compendium


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Optimisation of an analytical method for the determination of total fluoride in preservative-contaminated soils using water steam distillation and an ion-selective electrode
1999 - IRG/WP 99-20153
This paper describes a simple modified procedure for the quantitative fluoride determination of different origin in a soil matrix using a water steam distillation and an ion-selective electrode. Distillation methods generally require a preliminary preparation step like fusing. The modified method presented here is based on the direct distillation of fluoride so that no further sample preparation i...
E Melcher


The quantitative determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using TD-GC-MS
2001 - IRG/WP 01-20223
Last year we presented the paper (IRG/WP/00-20201) "Determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using GC-MS". Based on the intensive discussion at the meeting, the first experiences made with the calibration of the system for this application will be reported. For the quantitative determination of N-cyclohexyl-diazeniumdioxide in treated wood, milled m...
P Jüngel, J Wittenzellner, E Melcher


Rubberwood anatomy and its influence on gaseous permeabilit
1993 - IRG/WP 93-40005
The anatomical structure in several rubberwood (Hevea brasiliensis Muell. - Arg.) samples was examined by use of a Cambridge Stereoscan 600 scanning electron microscope. A series of electron micrographs is presented which illustrate those features anticipated as having an influence on permeability. A series of gas permeability experiments were performed on oven dried samples of rubberwood to deter...
A J Pendlebury, J A Petty


The accelerated L-joint test method for determination of the out of ground natural durability
1998 - IRG/WP 98-20146
The accelerated L-joint test incorporates a moistening device and uses a close end water trap in an open joint connection with a laminated tenon member consisting of the perishable reference wood species scots pine sapwood and beech. After one year of exposure it is possible to show a distinct identification of natural durability classes 4 and 5 against the more durable wood species. Both weight ...
J Van Acker, C Brauwers, M Stevens


Studies on the determination of the durability of wooden poles and fence posts
1982 - IRG/WP 3195
This study was carried out by the Forestry Research Institute. 5 Turkish main tree species, Oak (Quercus), pine (Pinus sylvestris), beech (Fagus orientalis) and Fir (Abies bornmülleriana) wooden poles and fence posts, were treated with Tanalith-U and creosote applying pressure process. Tanalith-U was applied by full-cell process and creosote was applied by empty cell process. Treated and untreate...
R Ilhan, O Taskin, A P Erten


An alternative method for the determination of lignocellulolytic enzymatic activities of white rot fungi
1998 - IRG/WP 98-10261
Some lignocellulolytic activities of wood decay fungi can be evaluated in an indirect way through the study of the decolorization that white rot fungi produces in culture media in the presence of dyes. In this assay, ten dyes were selected, which were added in concentrations of 0.00 1% - 0.003% (P/V) to four-day cultures of Trametes versicolor containing 1% of beech sawdust in a basal salt medium...
D Muñoz-Mingarro, F Llinares, F Rubio, M Yuste, C Rodríguez-Borrajo, J Jiménez, M T De Troya


Investigation of CCA fixation in wood by sequential extraction. I Determination of CCA component fixation and preliminary extraction results
2002 - IRG/WP 02-50188
The fixation of CCA-C preservative was investigated in sapwood of red pine (Pinus resinosa Ait.), trembling aspen (Populus tremuloides Michx.) and red maple (Populus tremuloides Michx.) at target retentions of 4.0, 6.4, 9.6 and 30.0 kg/m3. Treated wood sawdust was water extracted at close time intervals during the fixation and analyzed for the contents of unfixed hexavalent chromium, total Cr, Cu ...
S Radivojevic, P A Cooper


Determination of corrosive effect of liquid wood preservatives to metals – First experiences with a National Standard which is in revision
2006 - IRG/WP 06-20321
The development of standards is an essential tool to characterise different kind of materials and products. An important aspect during the development of a new product is to check the corrosion behaviour with other materials. Corrosion can cause several problems like pitting corrosion. Consequently the knowledge concerning the corrosive effect of liquid wood preservatives is important due to the s...
E Melcher


Determination of bis-(N-cyclohexyl-diazeniumdioxy)-copper in different matrices by photometer, thermal energy analyzer and HPLC
1999 - IRG/WP 99-20179
For the quantitative analysis of bis (N-cyclohexyl-diazeniumdioxy)-copper (Cu-HDO) three analytical methods are used. The employment of the different methods depends on the matrices involved. For several years now, the colorimetric determination of Cu-HDO by photometer has been applied to solutions and concentrates of wood preservatives. In principle, the technique consists of a quantitative conve...
J Wittenzellner, W Hettler, M Maier


Determination of fungitoxic value of preservatives in laboratory wood-block tests. Part 2: Statistical estimation
1989 - IRG/WP 2327
Laboratory modified agar-block tests were made to determine the fungitoxic value of the wood preservative CCA against the test fungus Serpula lacrymans using statistical methods. With the aid of statistical computer programmes based on the least square method. the regression equation was found for the dependence between sample mass loss and preservative retention both in terms of percentage and fo...
J Wazny, J D Thornton, K J Krajewski


Determination of fungitoxic value of preservatives in laboratory wood-block tests. Part 1: Standard procedures
1989 - IRG/WP 2326
By applying a modified agar-block method, a comparative analysis was made on the toxic value of the wood preservative CCA against the test fungus Serpula lacrymans. The procedure applied to determine the results accounted for different standards: EN (Toxic limit), ASTM (threshold retention), GOST (threshold retention and protection probability), PN (toxic doses) and JIS (value of efficiency). Desp...
J Wazny, J D Thornton


Inter-laboratory comparison of assessment methods for wood preservatives against subterranean termites: Determination of protection threshold limits for CCA
1999 - IRG/WP 99-10317
In 1996, several institutes conducted laboratory bioassays on the efficacy of unleached Pinus radiata specimens treated with copper-chromium-arsenic (CCA) and copper naphthenate (Cu Naph) at retentions of 0.5, 1.0, 2.0 and 4.0 kg/m3 (total salt for CCA; elemental copper for Cu Naph) against a range of species of subterranean termites (IRG/WP/96-10174). Each participant employed the standard test m...
J W Creffield, M Lenz


Evaluation of the permeability of fast grown wood species
1995 - IRG/WP 95-40042
The low natural durability of certain species of wood, implies the need for applying a protecting treatment to increase its life in service. Because of this, a knowledge of the permeability properties of the wood is desired. In this work, a simple and reliable method to evaluate the wood permeability is presented. For that, we have been used fast grown species, with low natural durability, Poplar ...
M T De Troya, A M Navarrete, E Sanchez, J E Garcia de los Rios, E L Rodríguez Trobajo


The association of bacteria with the increased permeability of water-stored spruce wood
1973 - IRG/WP 325
A microbiological investigation was undertaken to check our earlier work on patterns of bacterial counts and pH changes in water-stored wood. A survey of industrial activity was conducted upstream from the storage site with a view to explaining the existing bacterial flora. Further experiments were carried out with spruce bolts in enclosed tanks, using lake water with its natural bacterial flora a...
J A Dunleavy, J P Moroney, S E Rossell


Co-operative research project on L-joint testing. Sampling after 4 years exposure
1987 - IRG/WP 2274
In September 1983, Document No: IRG/WP/2208 was distributed giving guidance on sampling after 8 months exposure and including tables on which to record the test results. Similarly in September 1984, Document No: IRG/WP/2233 was distributed concerning sampling after 18 months exposure. No major problems have been notified to Princes Risborough Laboratory concerning the sampling method. It is theref...
J K Carey, A F Bravery


Determination of toxicity data for preservatives against Basidiomycetes by measuring the reduction in compression strength of wood
1988 - IRG/WP 2297
Blocks of Pinus radiata D. Don were treated to 12 retention levels with CCA and NaPCP. These were exposed for 12 weeks in agar jars to the dry rot (brown rot) Serpula lacrymans (Schum. ex Fr.) S.F. Gray. After mass loss determination, the same blocks were tested for reduction in compression strength parallel to the grain. Using both these parameters, together with interpolated 6 week strength loss...
J Wazny, J D Thornton


The resistance of timbers to impregnation with wood preservatives
1979 - IRG/WP 3137
It is anatomical structure which determines liquid flow rate within different timber species. This cannot be deduced from properties such as density or rate of growth, and can only be found by experiment. A standard test has been in use at the Princes Risborough Laboratory for many years, employing a pressure-impregnation treatment, and a large number of timbers have been studied. The test consist...
Anonymous


Permeability measurements on surface layers for detecting wood with abnormally high permeability
1988 - IRG/WP 2298
Wet storage of timber during the warm period of the year may lead to an increased permeability of the wood, an undesirable phenomenon for several wood industries and also for many end-uses. Neither before nor after drying, such wood with "wet storage damage" can be visually distinguished from wood with a normal permeability. A non-destructive method for inspecting the permeability of surface layer...
J B Boutelje, G Hägglund


The use of low cost X-ray fluorescence instruments in the determination of copper chromium and arsenic in preservative treated wood
1987 - IRG/WP 2278
Internal quality control in timber treatment plants can be pursued by analysis of preservative treatment solutions and treated timber. Treaters must proceed with costly and lengthy analyses through analytical laboratories. An alternative approach for the timber treater, is to use low cost analysers (L.C.A.'s) based upon x-ray fluorescence. Detailed comparisons have been made between stand...
J Norton, L E Leightley


Determination of thermal degradation of isothiazolone treated wood
1997 - IRG/WP 97-30154
Wood treated with 4,5-dichloro-2-n-octyl-4-isothiazolin-3-one was the subject of thermal degradation study. The study included burning isothiazolone treated wood under various temperatures with and without oxygen. The result showed that no harmful combustion products, such as polychlorinated dibenzo-p-dioxins, polychlorinated dibenzo-p-furans and polychlorinated biphenyls, were detected. These fin...
Bing Yu


A determination of the toxic level of ACQ2100 wood preservative for the powder post borer Lyctus brunneus (Stephens)
1994 - IRG/WP 94-20029
The sapwood of two Lyctus susceptible Australian hardwoods, messmate (Eucalyptus obliqua L'Herit.) and black bean (Castanospermum australe A. Cunn. et Fraser ex Hook) were pressure impregnated with ACQ2100, a wood preservative, to produce replicates of a range of retentions. Preservative retentions were determined by solution weight uptake at treatment and chemical analyses of selected sa...
A R Moffat


Mould growth and permeability in relation to wet-storage
1989 - IRG/WP 1414
The positive influences of wet-storage of roundwood to avoid attack by blue stain fungi and insects and to avoid cracking of wood during storage are well documented. Comparatively little information is, however, available on the effects on microbial susceptibility of the material after the storage period. The permeability of the wet-stored and the non-wet-stored material was determined. Wood block...
J Bjurman, E L Holappa


Amenability of radial permeability of Sitka spruce (Picea sitchensis (Bong.) Carr.) as affected by aspects of cell ends in uniseriate ray parenchyma tissue
2003 - IRG/WP 03-40252
The principal objective of this article was to recognise and understand the amenability of ray parenchyma cell ends (end platform) in uniseriate ray tissue to influence the radial permeability of Sitka spruce (Picea sitchensis (Bong.) Carr.) by examination of most (Queen Charlotte Islands in Rhondda, South Wales) and the least (South Oregon in Dalby, North-East England) seed origins that grown in ...
I Usta, M D C Hale


Changes in transverse wood permeability during the drying of rimu and radiata pine
1990 - IRG/WP 3636
When softwoods are dried and subsequently impregnated with waterborne preservatives two problems frequently occur, preservative screening of multi-salt preservatives and difficult re-drying. To study the causes, the permeability of rimu and radiata pine wood has been measured along the three principal directions. The radial and tangential permeabilities of the green sapwood of the two species were...
R E Booker


Quantitative Determination of Cyproconazole in Wood treated with Tanalith CY
2007 - IRG/WP 07-20369
The HPLC method has been widely applied to quantitative determination of cyproconazole in preservative solutions. However, HPLC assay has not been successfully employed to determine cyproconazole content in treated wood. Some extractives from treated wood hinder cyproconazole determination because they have a similar retention time to that of cyproconazole on an HPLC chromatogram. In addition, ...
I Momohara, T Miyauchi, M Mori


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