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Scanning Transmission X-ray Microscopy as a tool for examining chemical changes in wood cell walls due to enzymatic activity
2014 - IRG/WP 14-20556
As development of techniques for examining enzymatic activity on solid, complex biological materials, is considered to be an important factor in further development of enzyme applications and for understanding the decay of plant materials, this study explores applicability of Scanning Transmission X-ray Microscope (STXM) for determining chemical changes in enzymatically treated samples at the cell...
D Jeremic, R Goacher, R Yan, C Karunakaran, E R Master


Dynamic mechanical analysis (DMA) of nano cupric oxide (CuO) modified aqueous phenol formaldehyde (PF) resin
2014 - IRG/WP 14-40654
Phenol formaldehyde (PF) resins, modified by nano CuO incorporating alkane surfactant and polyvinyl alcohol (PVA) 17-99, were analyzed by dynamic mechanical analysis (DMA). The mechanical properties of its bonded plywood including tensile strength, modulus of rupture (MOR), modulus of elasticity (MOE) and shear strength under five test conditions were evaluated. Results indicated that the incorpor...
Wei Gao, Guanben Du


Full-scale impregnation of wood with siloxane using supercritical carbon dioxide
2014 - IRG/WP 14-40659
Full-scale impregnation of wood with siloxane was carried out using supercritical carbon dioxide as solvent. A batch of 3530 kg of Scots pine sapwood was impregnated to a retention of approximately 1.3% siloxane. The treatment also consisted of a simultaneous impregnation with organic biocides. The performance of the wood was evaluated in terms of capillary water uptake according to a modified EN ...
A Kjellow, F Imsgard, J Fernandes, R Wagner, J Delis


Termite resistance of wood modified with short- and long-chain siloxanes
2014 - IRG/WP 14-40660
Scots pine (Pinus sylvestris L.) sapwood specimens modified with short- and long-chain amino-functional siloxane emulsions were exposed to subterranean termites (Reticulitermes flavipes Kollar). Laboratory choice and no-choice tests following the standard EN 117 (2013) were conducted for 8 weeks in order to evaluate the influence of these silicon-based compounds on the termite resistance of treate...
P Gascón-Garrido, M-F Thévenon, H Militz, C Mai


Study of in-situ gel polymerization established by Si-O-Si framework within wood micropores
2014 - IRG/WP 14-40672
Sodium silicate was used to form Si–O–Si framework by gel process and optimize the effect of the methylolurea impregnation on poplar wood. The modifier cured within the wood micropores by in-situ gel polymerization during the kiln drying. The results showed that treated wood acquired higher mechanical strength, but lower hygroscopicity. New positions of the XRD peaks appeared which caused by s...
Zeng Bi, Qian Lang, Heyu Chen, Junwen Pu


Possible targets of wood modification in brown rot degradation
2014 - IRG/WP 14-40676
Wood modification protects wood from fungal degradation in a non-toxic manner. However, the mechanisms behind the decay resistance in modified wood are currently unknown. The aim of this study was to discuss the i) colonisation, ii) nutrient recognition, iii) transcription, iv) depolymerisation and v) hydrolysis steps in the brown rot degradation progress and explore whether they are inhibited by ...
R Ringman, A Pilgård, G Alfredsen, B Goodell, K Richter


Interpretation of moisture monitoring data - Relevance of moisture content thresholds for fungal decay
2015 - IRG/WP 15-10839
It is widely accepted that besides temperature wood moisture content (MC) is the key factor when it comes to durability of wooden structures exposed to weathering. Many approaches to predict the service life of wooden structures have therefore been based on using wood MC as one major input-variable to develop dose-response relationships between material climate and decay response. However, to impr...
L Meyer, C Brischke


Introduction of the COST FP 1303 Cooperative Performance Test
2015 - IRG/WP 15-20567
COST Action FP 1303 “Performance of bio-based building materials” successfully started in October 2013 and an ambitious program was set up for the four year programme. COST Actions provide an excellent opportunity for collaborative research, e.g. in the frame of Round Robin tests. The idea of this respective test was to distribute a fairly simple test set up to as many places in Europe as poss...
M Humar, C Brischke, L Meyer, B Lesar, N Thaler, D Jones, S Bardage, C Belloncle, J Van den Bulcke, J M Abascal, G Alfredsen, D Baisch, B Brunnhuber, G Cofta, E Grodås, E Frühwald Hansson, M Irle, H Kallakas, J Kers, M Klamer, P Larsson Brelid, A B Maider, K C Mahnert, E Melcher, R Möller, M Noël, L Nunes, G A Ormondroyd, S Palanti, N Pfabigan, A Pilgård, A O Rapp, P Schumacher, E Suttie, T Teppand, M Touza, J Van Acker


Effect of natural variability of European Oak wood on heat treatment process and potential implication on wood durability
2015 - IRG/WP 15-40693
Environmental pressures appeared in France and in most European countries during the last decade has led to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative method during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


How does the test methodology influence the outcome of durability testing of thermally modified wood
2015 - IRG/WP 15-40699
Thermally modified wood is commercially available on the European market since many years. Today, many production units with various production capacities and different modification processes exist. Industrial scale wood heat treatment processes, under the trade name of ThermoWood were developed in Finland. ThermoWood has two standard treatment classes with different target properties, namely Ther...
A Gellerich, S Bollmus, H Militz


Polyamidoamines (PAA) functionalized with siloxane fragments as potential wood preservatives
2015 - IRG/WP 15-40708
Polyamidoamines (PAAs) utilized in this research were obtained by the reaction between N,N-methyl-bis-acrylamide (MBA) and Ethanolalmine (EtA) and/or aminopropytriethoxysilane (APTES). Different combinations between them were tested as wood preservatives against fungal decay. First, in situ impregnations of PAAs, with the reagents above described in different ratio, were performed and the effectiv...
S Palanti, G Predieri, E Feci, L Bergamonti


High-frequency monitoring of mass loss due to brown rot degradation of modified wood
2016 - IRG/WP 16-10862
Fungi growing in liquid culture undergoes three separate phases in which they i) adapt to the new environment, ii) grow unrestrictedly and exponentially, and iii) are inhibited to increase in number/mass due to lack of nutrients etc. Filamentous fungi have been shown to exhibit similar growth phases in a solid food substrate and have been modelled to grow in this way also in solid wood. In modifie...
R Ringman, A Pilgård, K Richter


Susceptibility of wood substrates to Aurebasidium pullulans at different temperatures
2016 - IRG/WP 16-10863
There is an increasing awareness of how the aesthetical performance of wood exposed outdoors changes over time and especially in the first few years after installation. Mould and blue stain fungi are biological agents that contribute to the weather grey colour on a wooden façade, and the blue stain fungi Aureobasidium pullulans is commonly identified as colonizer on coated and uncoated wood expos...
L Ross Gobakken, G Alfredsen


Selection of most aggressive test fungi for modified wood - Practical laboratory experience
2016 - IRG/WP 16-20579
One main objective of wood modification processes is the improvement of the durability against wood destroying organisms. Therefore, investigations of the resistance against wood destroying fungi have been one of the main focus within the last years. For the interpretation of the durability results, the selection of suitable test fungi is one of the main questions. A “wrong” fungus species may...
A Gellerich, S Bollmus


Measurement of Cell Wall Moisture in Acetylated Radiata Pine Using Low-Field Nuclear Magnetic Resonance
2016 - IRG/WP 16-20583
Understanding the interaction of water with acetylated wood is necessary to explain how the protective mechanism of acetylation functions. Low-field nuclear magnetic resonance is one technique for assessing water in wood. Pinus radiata earlywood sapwood samples were acetylated to various weight percentage gains and then analysed with this method. Increased levels of acetylation showed significantl...
H G Beck, C A S Hill


How intraspecific radial variability of the European Oak’s may influence mild pyrolysis process and durability of the material
2016 - IRG/WP 16-40725
Last decades wood is promoted as building material. Unprotected wood exposed to outdoor conditions undergoes a variety of degradation induced essentially by fungi attacks. Heat treatment of wood by mild pyrolysis (180°C T 240°C under inert atmosphere) is a preservation process with a weak environmental impact, and therefore, is viewed as an interesting alternative to the chemical impregnation me...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


Role of cell wall specific moisture content on the brown-rot fungal attack on wood
2016 - IRG/WP 16-40736
Wood is a hydroscopic resource because the cell wall polymers contain hydroxyl and other oxygen-containing groups that attract moisture through hydrogen bonding. Moisture content varies with changing moisture content in its environment. The moisture content in wood is responsible for many of the performance properties we observe. The strength properties of wood are dependent on the moisture con...
R M Rowell


Durability of Thermally Modified Engineered Wood Products
2016 - IRG/WP 16-40745
In this study, rated plywood, oriented strand board (OSB), laminated strand lumber (LSL), and laminated veneer lumber (LVL) were thermally modified as a post-treatment at 140 °C, 150 °C, 160 °C, 170 °C, and 180 °C using a closed, pressurized treatment method. Eastern larch OSB manufactured from heartwood and sapwood was also thermally modified as a post-treatment at 160 °C and 180°C. All ...
H M Barnes, M D Aro, A Rowlen


Development of a new method for wood hydrophobizing and fixation of copper compounds by chemical hardening of vegetable based modified oils
2016 - IRG/WP 16-40754
Wood products with ground and direct water contact, but without sufficient biological durability, have to be protected against biological degradation by fungi and other microorganisms. Due to European legislation (Biocidal Products Regulation 528/2012), the selection of possible chemical agents, which are still allowed to be used, is diminishing rapidly. The use of previously widely applied, very ...
C Swaboda, M Fischer, K Jacobs


Marine Borer Resistance of Acetylated and Furfurylated Wood – Results from up to 16 years of Field Exposure
2016 - IRG/WP 16-40756
Furfurylated and acetylated Scots pine sapwood has been tested since 1999 in a marine field with high marine borer activity. In 2004, two test groups with acetylated southern yellow pine (product later known as Perennial Wood™) were put out and over the whole test period differently furfurylated wood (later marketed as Kebony®) test groups have been started. Furthermore, some combinations of mo...
M Westin, P Larsson Brelid, T Nilsson, A O Rapp, J P Dickerson, S Lande, S Cragg


Accelerated weathering and fungal resistance of wood modified with isopropenyl acetate
2016 - IRG/WP 16-40764
Chemical modification of Rubberwood (Heveabrasiliensis Müll.Arg) with isopropenyl acetate (IPA) in presence of anhydrous aluminum chloride and iodine as catalysts was carried out. Modified wood surfaces were exposed to UV light source in an accelerated weathering tester to evaluate UV resistance. Anti-swelling efficiency (ASE) and fungal resistance of modified wood were also evaluated. Modified w...
G B Nagarajappa, K K Pandey


State of the art of industrial wood protection in Portugal
2016 - IRG/WP 16-30703
This work intended to give a perspective of industrial wood protection in Portugal. A survey was made of the companies treating wood mainly for use classes 3 and 4 such as autoclave treatments with biocides and wood modification procedures. Currently there are 23 companies with 33 production plants with an autoclave installed for wood preservation by impregnation. There are also two companies prod...
L Nunes, J Carmo, J Vicente, B Esteves


10 year Report on COST E37 Round Robin Tests – Comparison of results from laboratory and field tests
2017 - IRG/WP 17-30718
A round robin involving 15 European participants was set up in 2006. The round robin consisted of both a field test according to the double layer test method and a laboratory test with two different preconditioning methods. The laboratory test results were reported in an earlier IRG paper (IRG/WP13-20535) but are included also in this paper in order to facilitate the comparison with the field test...
M Westin, E Conti, J Creemers, P-O Flæte, A Gellerich, I Irbe, M Klamer, E Melcher, R Moeller, L Nunes, S Palanti, L Reinprecht, E Suttie, H Viitanen


COST FP 1303 Cooperative Performance Test – Results after two years outdoor exposure
2017 - IRG/WP 17-20620
COST Action FP 1303 ‘Performance of Bio-Based Building Materials’ started in October 2013 and an ambitious program was set up for four years. Among this a collaborative field test was planned. The idea of the cooperative performance test was to distribute a fairly simple test set up to as many places in Europe as possible in order to collect performance data reflecting the full range of climat...
B Lesar, M Humar, C Brischke, L Meyer-Veltrup, D Jones, N Thaler, J M Abascal, G Alfredsen, B Brunnhuber, E Grodås, M Irle, J Kers, M Klamer, K-C Mahnert, E Melcher, S Palanti, M Noël, E Suttie, N Pfabigan, M Touza


Moisture content as a quality control parameter in thermally modified timber production
2017 - IRG/WP 17-20622
Quality assurance (QA) or factory production control (FPC) is necessary to ensure a proper production process. The requirements of QA/FPC can result from EN and national standards, quality assurance systems, or producer-specific rules. TMT producers must ensure that the process was correct, and to ensure traceability of products. In addition to the electronic records, the material should be che...
W Scheiding, H Turkulin, S Stein


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