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A reliable spot test for TCMTB in wood
1992 - IRG/WP 92-2391
Test specimens of slash pine (Pinus elliottii) and spotted gum (Eucalyptus maculata) were treated with aqueous emulsions of Busan 30WB and Busan 31, containing the fungicide TCMTB (2-(Thiocyanomethylthio)benzothiazole), or with solutions of TCMTB in toluene. These and matching untreated specimens were subjected to a wide range of procedures in an attempt to reveal TCMTB penetration patterns. Most ...
D E Ferlazzo, M J Kennedy


Trial to determine a suitable schedule for radial and longitudinal treatment of plug samples by comparison of changes in the fluid retention and the treated area
2001 - IRG/WP 01-40211
A full-cell process was carried out using different treatment schedules for radial and longitudinal samples because of the anisotrophy of flow. When timbers are impregnated with preservatives much better penetrations are obtained via the end grain than laterally (across the grain). Therefore, suitable schedules for radial and longitudinal flow directions were determined in an trial experiment usin...
I Usta


Application of energy dispersive X-ray fluorescence spectrometry to the quantitative analysis of organotin preservative solutions and treated wood
1978 - IRG/WP 3125
One technique frequently used for the quantitative analysis of material containing inorganic compounds is energy dispersive X-ray fluorescence spectrometry. It has been shown previously that this technique can be readily used to determine the retentions of chromated copper arsenate and ammoniacal copper arsenate treated wood. This paper reports the results of a preliminary study to determine wheth...
J N R Ruddick


International collaborative laboratory comparison of two wood preservatives against subterranean termites: Update
1994 - IRG/WP 94-20032
It was agreed by members at the termite workshop at the 24th annual meeting of IRG in Orlando, USA, in May 1993 to initiate an international subterranean termite laboratory bioassay to compare the various preferred termite protocols used by IRG termitologists. The author was nominated to co-ordinate this comparative laboratory evaluation of two wood preservatives (CCA and Cu-naphthenate) against t...
J R J French


A comparison between different accelerated test methods for the determination of the natural durability of wood
1996 - IRG/WP 96-20099
According to the European standard EN 350-1 the natural durability of wood is defined as: "the inherent resistance of wood to attack by wood destroying organisms". This standard also describes how, for certain hazard classes, the durability is determined. The two methods described in this standard are the kolleflask method (EN 113) and the field-stake-test method (EN 252). The EN 113 test gives re...
H Militz, S G L Michon, J E Polman, M Stevens


Toxic value estimation of wood preservatives by using the probit analysis
1990 - IRG/WP 2348
As it was assumed from previous experiments, the probit analysis appears to be the most suitable method of all used to estimate the toxic value of wood preservatives. With the help of the classical agar-block method the probit analysis was tested for its suitability in: 1) fungitoxic value estimation of the WR-3 preservative (quaternary ammonium compound + borate), as compared to different test fu...
J Wazny, K J Krajewski


Non-destructive stress wave measurement of decay and termite attack in experimental wood units
1986 - IRG/WP 2256
The purpose of this study was to determine if stress wave analysis could be used to monitor the degradation of wood specimens exposed to the brown-rot decay fungi (Gloeophyllum trabeum) and of wood specimens subjected to attack by subterranean termites. One hundred fifty 3/4 by 3/4 by 12 in. Southern pine specimens were used for exposure to brown-rot decay fungi and two hundred twenty-five 3/4 by ...
R F Pellerin, R C De Groot, G R Esenther


Comparison of methods for monitoring CCA fixation
1994 - IRG/WP 94-40023
The CCA fixation status in the outer 12.5 mm of pole sections of southern pine (Pinus sp.), red pine (Pinus resinosa) and lodgepole pine (Pinus contorta var. latifolia) were followed during fixation at 21°C under non-drying conditions by the following procedures: - Qualitative CrVI indication by the chromotropic acid spot test. - Quantitative CrVI in the expressate by the diphenylcarbazide method...
P A Cooper, Y T Ung, G Zanjani


A comparison of the migration behaviour in soil of different waterborne wood preservatives and their leachates
1997 - IRG/WP 97-50091
Lysimeter tests were carried out on water-soluble wood preservatives and on wood preservative components leached out of impregnated wood. The purpose of these tests was to determine the extent to which the migration behaviour of environmentally relevant ions in the soil is influenced under comparable conditions. The results clearly show that the groundwater is especially at risk when wood preserva...
E Melcher, R-D Peek


Leachability of didecyldimethylammonium chloride (a quaternary ammonium compound) from four wood species
1982 - IRG/WP 3204
Sapwood blocks prepared from red pine, ponderosa pine, southern yellow pine and hem-fir (a commercial mixture of western hemlock and amabilis fir) were treated with didecyldimethylammonium chloride, (an alkylammonium compound, AAC). After oven drying the blocks were vacuum impregnated with distilled water and subjected to a static leach cycle for 48 hours. The leachate was analyzed and the amount ...
J N R Ruddick, A R H Sam


Preliminary PIXE micro-analysis of copper-chrome-arsenic preservative treated Malaysian hardwoods
1999 - IRG/WP 99-20169
The novel nuclear microscopy, essentially the Particle-induced X-ray Emission (PIXE) system, was applied for examining the macro-distribution and micro-analysis of copper-chrome-arsenic (CCA) preservative in Malaysian hardwoods Koompassia malaccensis, K. excelsa, Alstonia spp. and Dipterocarpus spp., and one temperate pinewood Pinus sylvestris, where the preservative retention differed between the...
A H H Wong, R B Pearce, G W Grime, F Watt


Comparison between two laboratory test methods for determining the effectiveness on wood preservatives against blue stain in fresh wood
1987 - IRG/WP 2289
Most of the work done on determination of the effectiveness of new formulae for treating fresh wood against blue stain have been focussed on their use in the manufacture of saw timber. This work explains two laboratory methods, one which simulates the working and climatological conditions of factories making packages for fruit and vegetables in the Spanish Levante, showing that contamination of wo...
A M Navarrete, M T De Troya


The quantitative determination of quaternary ammonium compounds in treated timber – results of an extended ring test
2002 - IRG/WP 02-20240
The determination of quaternary ammonium compounds (QAC) by means of a 2-phase-titration or photometry is a well established procedure for the quantification of cationic detergents in aqueous solutions. It is known that this analytical principle can also be used for the measurement of QAC extracted from treated timber. However only few information are available concerning the reproducibility or th...
E Melcher, C Bornkessel, J Gunschera, R Hamberg, H Härtner, H-N Marx, U Schoknecht, J Wittenzellner


Natural durability transfer from sawmill residues of white cypress (Callitris glaucophylla). - Part 4: Analysis of extracts and treated wood for active components
2000 - IRG/WP 00-20215
In order to facilitate the commercial implementation of a large project aimed at recovering 'waste' durability components from sawmill residues of Callitris glaucophylla, it has been essential to develop analytical methodology for the important bioactive components of the heartwood extract. This methodology will be used 1) to standardise the activity of successive production batc...
Hui Jiang, M J Kennedy, L M Stephens


Fungal colonisation of the keelson and associated structures of a nineteenth century wooden frigate: Concepts of community structure and development
1994 - IRG/WP 94-10072
The early stages of microbial colonization and succession of wooden surfaces exposed to the sea have been extensively studied as have the community structures of archaeological timbers subjected to submergence and then retrieval from the sea. The frigate UNICORN, a largely intact 19th century wooden ship based in Dundee, Scotland, provides the microbial ecologist with a unique opportunity to study...
N A White, J W Palfreyman, G M Smith


Detection of wood decay fungi in wood using a PCR-based analysis
1998 - IRG/WP 98-10279
We have developed a DNA-based assay to reliably detect brown rot and white rot fungi in wood at different stages of decay. DNA, isolated by a series of CTAB and organic extractions, was amplified by the polymerase chain reaction using published universal primers and basidiomycete-specific primers derived from ribosomal DNA sequences. We have surveyed 7 species of brown rot fungi, 7 species of whit...
C Jasalavich, A Ostrofsky, J Jellison


Determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using GC-MS
2000 - IRG/WP 00-20201
Beside the biological effectiveness the approval of a chemical wood preservative requires also techniques for the analytical determination of active ingredients in different matrices. Fulfilling of the last requirement is particularly difficult in the case of impregnated timber treated with wood preservatives containing organic compounds. This paper describes a procedure for the determination of t...
P Jüngel, J Wittenzellner, E Melcher


Surface retentions of PCP, TCMTB and MTC obtained during a field trial of antisapstain formulations
1993 - IRG/WP 93-20002
Formulations containing NaPCP or TCMTB and MTC were included as reference products in a recent field trial of antisapstain formulations in Queensland. Retentions of these actives on the surface of treated sawn Pinus elliottii were monitored by ultrasonic solvent extraction of excised samples and analytical determination by high performance liquid chromatography. Distribution of actives with depth ...
D E Ferlazzo, M D Needham, M J Kennedy


IRG/COIPM INTERNATIONAL MARINE TEST - to determine the effect of timber substrate on the effectiveness of water-borne salt preservatives in sea-water. Progress Report 3: Report of first inspection of samples at Lae, Papua New Guinea
1978 - IRG/WP 446
Samples for the international marine test were placed on frames numbered I to VII. Frames numbered VII of both CCA and CCB trials are being stored dry in the laboratory at F.P.R. & D.C. Frames I to VI of both trials were suspended in the sea at Lae Harbour (Morobe Province, Papua New Guinea) on 6th December 1977. The first inspection of the CCA trial was carried out on 8th June 1978, at which ...
S M Cragg, C R Levy


Comparison of performance of wood preservatives in laboratory and field tests of treated commodities
1993 - IRG/WP 93-20010
The purpose of laboratory tests for evaluating efficacy of wood preservatives is usually to establish toxic values against standard strains of wood decay fungi. Exposure conditions are usually chosen as optimal for fungal growth. Toxic values so determined serve as a guide as to expected performance of the preservative in field stake tests or in above ground exposure tests. Test material is select...
M E Hedley


Determination of boron levels in solution and in treated wood
1994 - IRG/WP 94-20041
Four methods of measuring boron levels in solutions were investigated. The methods compared included the azomethine-H method which is commonly used in soils and plant tissues, the methods outlined in the Australian Standard AS 1605 (1974) and in Wilson (1958), and the atomic absorption spectrophotometry method. Defect-free radiata pine (Pinus radiata D. Don) sapwood and wood flakes were treated to...
F J Romero, P Vinden, P Kho


Comparison of variable, constant and fluctuating pressure methods
2001 - IRG/WP 01-40212
The objective of this work was to evaluate potential improvements in pressure treatment arising from the use of a control valve. A constant pressure of 1035 kPa was compared to the conventional variable pressure method where the pressure is allowed to drop to 860 kPa as the solution is absorbed by the wood. A fluctuating pressure method (FPM) where the pressure cycles between 1000 and 1070 kPa was...
S M McFarling, P I Morris


The remaining concentration of inorganic wood preservative components in EN 252 stakes after ground contact
2000 - IRG/WP 00-50159
In order to determine the biological efficiency and the remaining concentration of different inorganic and organic active ingredients during service, EN 252 specimens were impregnated with 3 copper based wood preservatives. The stakes were installed in the test field of the DESOWAG GmbH, Rheinberg, for at least 7 years. At the end of the field test some of these stakes were divided into 10 uniform...
E Melcher, H-W Wegen


Comparison of the FRIM and forest research laboratory methods for screening of anti-sapstain formulations
1999 - IRG/WP 99-20170
Two laboratory methods for screening of anti-sapstain formulations were compared. The method adopted by the Forest Research Institute Malaysia (FRIM) involved 3 weeks assessment of rubberwood (Hevea brasiliensis) blocks, dipped in the candidate formulation and inoculated with mycelial/spore suspension of sapstain (Botryodiplodia theobromae) or decay (Schizophyllum commune) fungi, and incubated on ...
A H H Wong, D R Eden, C M Chittenden, M E Hedley, R N Wakeling


Susceptibility of antisapstain fungicides to rain wash-off
1994 - IRG/WP 94-30046
Results of trials using miniature timber packets and simulated rain wash-off are described. Six fungicidal actives in five commercial antisapstain formulations were involved, and a clear influence of rainfall timing after antisapstain treatment was demonstrated. Differences between actives and formulations were most marked where water-spray was applied in the first hour after treatment, though eve...
R N Wakeling, D J Cross, D R Eden, P N Maynard


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